2008-06-15 22:32:55
/ 分析&测试技术
KNO3的纯度检测根据usp的方法检测但是发现结果滴定不出来,即根本没有KNO3 。如下为USP方法:Assay— [note—Use water that is carbon dioxide- and ammonia-free.]Cation-exchange column— Transfer strongly acidic styrene-divinylbenzene cation-exchange resin (16- to 50-mesh) to a 2-cm diameter chromatographic column to a depth of about 20 cm.Procedure— Dissolve about 400 mg of Potassium Nitrate, accurately weighed, in 100 mL of water. Pass this solution through the Cation-exchange column at a rate of a.
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